Case Study
Case Study
Case Study
Case Study
Case Study

Fully-Automated Pilot-Scale Polystyrene Monomer Dosing Station

for operating with highly-viscous polymer.
The task

A pilot-scale high-impact polystyrene pilot plant on a very limited budget

One of ILS oldest clients came with a request for a pilot-scale high-impact polystyrene pilot plant. The group had very little in-house experience in this area but had had extensive experience working with ILS in a number of other areas. The ever-increasing world demand for HP-polystyrene is a major driver for further development in this area.
The ILS solution

A design that met the clients needs and still fit in a very limited budget

The highly-explosive styrene and ethylbenzene feedstocks had to be stored in a separate building in an explosion-proof certified operating space. ILS designed the feedstock storage and dosing modules to be fully explosion proof adhering fully to our clients stringent specs.

The reaction section had to operate with highly-viscous polymer. This required powerful stirring and ILS went one step further and incorporated torque sensors, which proved extremely valuable to the client as an on-line tool for judging product quality. The unit was fitted with a powerful, dynamic Lauda thermostat system which made possible execution of polymerization reactions within the tight temperature specs, which were demanded by our client.

Removal of viscous polymer melt without blockage required double-jacketed heated tubing and flanges. High-temperature gear-pumps were implemented in a dead-volume-free configuration on the bottom of the reactors to allow for polymer melt to be removed at the end of reaction and continuously fed to a high-temperature vacuum devolatizer where unconverted monomer could be removed to extremely low levels. The entire unit fit in a very small space as the client only had a small, exiting test cell for the unit. The process-control hardware and software was designed 100% in accordance with the clients site standards (Siemens/iFix).

The result

A very challenging project successfully completed

Numerous bugs had to be overcome after delivery as ILS did not yet have chemical validation testing capability at that time. We are proud of the fact, however, that ILS was able to successfully complete the site acceptance for this extremely challenging project. We have since continued to do business with this valued ILS client.
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